(3a R ,6 R )-3,3,6-Trimethyl-3,3a,4,5,6,7-hexahydro-2 H -indazole-2-carbothioamide

Abstract : The title compound, C11H19N3S, was prepared by the reaction of (R)-pulegone with thio­semicarbazide in acidic medium, using ethanol as solvent. The mol­ecule is built up from fused six and five-membered rings. The six-membered ring adopts a chair conformation, while the five-membered ring displays an envelope conformation with the dimethyl-substituted C atom as the flap. The dihedral angle between the mean planes of the two rings is 20.35 (6)°. In the crystal, mol­ecules are linked by N-HN and N-HS hydrogen bonds into chains running parallel to [100].
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https://hal.univ-reims.fr/hal-02430290
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Submitted on : Tuesday, January 7, 2020 - 11:22:06 AM
Last modification on : Wednesday, January 8, 2020 - 2:02:49 AM

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Abdellah N'Ait Ousidi, My Youssef Ait Itto, Aziz Auhmani, Abdelkhalek Riahi, Sylviane Chevreux, et al.. (3a R ,6 R )-3,3,6-Trimethyl-3,3a,4,5,6,7-hexahydro-2 H -indazole-2-carbothioamide. IUCrData, 2016, 1 (4), ⟨10.1107/S2414314616005733⟩. ⟨hal-02430290⟩

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